Crystal structure of 3-[(3-oxo-1,3-dihydro-isobenzofuran-1-yl)-phenethylamino]- 2-phenethyl-2,3-dihydro-isoindol-1-one, C32H28N2O3

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2-Benzyl-3-hy­droxy-3-methyl-2,3-dihydro-1H-isoindol-1-one

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In the title compound C18H20N2O2, the morpholine ring adopts a chair conformation with the exocyclic N-C bond in an equatorial orientation. The N atom of the morpholine ring and the C atom of the carbonyl group are in an anti conformation about the central C-C bond [torsion angle = -162.92 (11)°] and the dihedral angle between the planes of the benzene ring and the pyridine ring is 83.30 (5)°. ...

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4-[(3-Oxo-1,3-dihydro-2-benzofuran-1-yl)amino]­benzoic acid

In the title compound, C(15)H(11)NO(4), the dihedral angle formed by the benzene ring and the essentially planar 2-benzofuran ring system is 55.93 (3)°. In the crystal, inter-molecular O-H⋯O hydrogen bonds link pairs of mol-ecules, generating centrosymmetric R(2) (2)(8) ring motifs. These dimeric units are connected via N-H⋯O hydrogen bonds, forming C(6) chains along [100].

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ژورنال

عنوان ژورنال: Zeitschrift für Kristallographie - New Crystal Structures

سال: 2003

ISSN: 2197-4578,1433-7266

DOI: 10.1524/ncrs.2003.218.1.81